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Wilmad-LabGlass, MMS-005B, 5mm Shigemi Tube Set, 8mm Bottom, CD3OD, Bruker
Shigemi tube features a susceptbility matched bottom and plunger for each of the following solvents: CDCL3 CD3OD D2O DMSO-d6 This feature would effectively reduce the boundary gradients at the edges of the coil. Therefore, it is no longer critical to keep the general NMR sample rule as "sample height = 3 times the coil length".
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